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400 MHz NMR Spectrometer

Workplace of device "400 MHz NMR Spectrometer"
Workplace: Regional Centre of Advanced Technologies and Materials
Faculty: Faculty of Science - Regionální centrum pokročilých technologií a materiálů
Street: Šlechtitelů 11
City: Olomouc
Characteristic of workplace: The main objective of the Regional Centre of Advanced Technologies and Materials (RCPTM) is the regular transfer of the developed high-tech technologies into the medicinal, industrial and environmental practice and the participation of the Centre in the prestigious international networks and consortia. RCPTM focuses predominantly on the top research in the metal oxide nanoparticles for catalytic and magnetic applications, carbon nanostructures, metal nanoparticles for antimicrobial and water treatment technologies, coordination chemistry, photonics, new instrumentation in optics and analytical chemistry. One of the main goals is also to offer the first-rank microscopic, spectroscopic, magnetic and other devices for the commercial utilization.
Device "400 MHz NMR Spectrometer"
Manufacter Varian, Inc.
Number of pcs. 1
Year 2008
Usage Measurements of high-resolution spectra of the studied sample solutions: direct measurements of e.g. 1H, 19F, 13C, 15N, 29Si, 31P or 119Sn (with 1H or 19F heteronuclear decoupling), 1H homonuclear decoupling (e.g. NOEDIFF), homonuclear correlation (e.g. COSY, TOCSY, INADEQUATE), NOE experiments (e.g. NOESY, ROESY), heteronuclear correlation (e.g. DEPT, APT, HETCOR) and experiments with indirect detection (e.g. HMQC, HMBC, HSQC, HSQC-TOCSY, HSQC-TOCSY).
Specification
  • Magnet: 9.4 T, internal diameter 54 mm, 400 MHz
  • linear 2-chanel RF system with a high dynamic range
  • preamplifier for 1H/19F and broadband preamplifier for 109Ag – 31P
  • Probes: 1H/19F/13C/31P/15N 5mm AutoSwitchable and 1H-19F{15N-31P} 5mm OneNMRTM PFG with a manual or automatic choice of the measured nucleus with a temperature interval from -80 to 130 °C
  • NMR Software with an automatic function of lock, shim, phase, receiver gain, rotation, insert and removal of the sample
Extern No
Přesun No
Category of "400 MHz NMR Spectrometer"
"Inorganic chemistry", "Analytical chemistry, separation", "Macromolecular chemistry", "Biochemistry", "Physical chemistry and theoretical chemistry", "Electrochemistry", "Industrial chemistry and chemical engineering"